osmium tetroxide fixation

From: Jan_F_Keij@sbphrd.com
Date: Fri Jun 22 2001 - 17:28:51 EST


Folks,

In a effort to quench peritoneal macrophage autofluorescence, I resorted to
OsO4 fixation and ended up with a mixed bag.  I realize that there
alternative approaches to the problem of high autofluorescence, but this is
the approach I have chosen for at the moment.

Procedure
Murine peritoneal cells were harvested, washed and incubated with B220-FITC
and CD3e-PE, washed again and then either (A) incubated directly in OsO4
(0%, 0.1%, 0.2%, 0.5%, 1%, 2%) in PBS, or (B) first fixed in 1%
formalin-PBS (60' in ice, 1 wash with PBS) and then incubated with OsO4.
All samples were diluted 1/4, centrifuged and washed 1x with PBS.

Results
At 0.1% OsO4 in PBS, the autoflu is almost as low as for viable unfixed
lymphocytes.  However, most of my CD3 and B220 signal intensities are also
lost.  Several washes did not yield a return of my FITC and PE signals.  I
got the same results with and without pre-fixation.

Questions
Not being familiar with OsO4, I'd like to hear from those of you who are.
? Did I quench my fluorochromes (irreversibly?), did my Ab's "fall off", or
was my Ag-Ab complex stripped from the surface?
? Would I stand a chance of better results if I were to incubate with the
Ab's after the fixation?
? In case of Ab/Ag-Ab losses, would glutaraldehyde fixation be a more
"powerful" fix?  (I am aware of > autoflu by glutaraldehyde)

I'll summarize the responses and their effect on my experiments.

Thanks,

Jan.

GlaxoSmithKline
Cytometry Resource
709 Swedeland Road
King of Prussia, PA19604
(610)-270-4183



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