paraformaldehyde vs formaldehyde

From: DARZYNKIEWICZ ZBIGNIEW (DARZYNK@nymc.edu)
Date: Fri May 21 1999 - 13:51:48 EST


Paraformaldehyde is a polymerized form formaldehyde. It is hardly soluble
and it cannot be used as a fixative. Only formaldehyde is used as a
fixative.  Howeve, formaldehyde in aqueous solutions spontaneously
polymerizes. Therefore, methanol is often added to slowdown the
polymerization reaction. Solutions of formaldehyde (usually ~ 37%) in water,
containig 10-15 % methanol as a preservative are generally called
"formaldehyde"; such solutions are being sold by most reagent companies.
Solutions further diluted (4-10 %) received name "formalin". 
Methanol-free formaldehyde, which sometimes is preferred (e.g. for fixing
cells for some some histochemical  reactions or in immunocytochemistry), can
be obtained by hydrolysis of paraformaldehyde. This is usually done by
extensive heating of paraformaldehyde solutions. Because of this procedure
the methanol-free formaldehyde received (incorrrectly) the name
"paraformaldehyde". In the past, this was the most common way to obtain
methanol-free formaldehyde. Unfortunately, this incorrect name  is still
often used in the literature, generating the confusion. The methanol-free
formaldehyde solutions can now be purchased. Some are called "ultrapure". We
purchase such solutions (10%) from Polysciences, Inc. (800-523-2575); they
can be stored at room temperature. I would not recommend, however, to store
them longer than one year, since formaldehyde in these solutions still has
tendency to polymerize. It should be noted that all formaldehyde solutions
are highly toxic and carcinogenic.
Zbigniew Darzynkiewicz 



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