Re: Miltenyi magnetic beads and CD34+

From: D. Robert Sutherland (rob.sutherland@utoronto.ca)
Date: Mon Oct 22 2001 - 18:46:52 EST


Hi Denice Hong and Paul Weiss,

Before specifically addressing the original questions, it is important
to note that the CD34 antibody used in the Miltenyi device is the class
II epitope-specific monoclonal antibody QBEnd10 and NOT (as Paul
suggested) the class III epitope-specific antibody 8G12 (commercially
known as 'HPCA2' from BD Biosystems).  The QBEnd10 epitope is located at
the far N-terminus of the 'flag-pole-like' CD34 molecule.  This epitope
is composed of a linear stretch of 6 to 8 amino acid residues and as
such is expressed on all glycoforms of the mucin-like CD34
glycoprotein.   Again, in contrast to Paul's suggestion, it is NOT
possible to assess the purity of the selected CD34+ cells with 'HPCA-1'.
There are several reasons for this:

First, HPCA-1 (aka clone My10), detects a class I (sialic
acid-dependent) epitope (also in the far N-terminus) on CD34.  As such,
it probably cannot detect all glycoforms of the mucin-like CD34 molecule
on all cells that express them. Furthermore, since My10's binding to
CD34 depends at least in part on the presence of specific negatively
charged sialic acid residues, its conjugation with similarly negatively
charged fluorochromes such as FITC efffectively destroys its already
weak binding affinity for its epitope. Additionally, the class II
epitope is 'nested' within the class 1 sialic acid dependent epitopes at
the far N-terminus of the CD34 molecule and even if it were possible to
conjugate the class 1 antibodies such as My10 with large (non-charged)
fluorochromes such as phycoerythrin, the presence of QBEnd10 (and
paramagnetic beads) sterically hinder the binding of large
macromolecular complexes such as antibody:PE conjugates.

So, what can be used?  Class III epitope-specific antibodies are used
since they detect a 'common' non-glycosylation-dependent epitope of
CD34.  The class III epitope(s) are sufficiently spatially separated
from the class I and class II epitopes that 'orbital steering' (the
Lunar equivalent of steric hinderance) is not a problem.   Furthermore,
they can be conjugated with a variety of fluorochromes without loss of
high avidity binding. Recommended reagents include clones 581 (from
Beckman-Coulter) and HPCA-2.  These issues have been detailed is several
publications (The CD34 antigen: Structure, biology and potential
clinical applications. J. Hematotherapy, 1: 115-129, 1992,  The ISHAGE
Guidelines For CD34+ Cell Determination By Flow Cytometry. J.
Hematotherapy 3:  213-226, 1996, Structural and functional features of
the CD34 antigen: an update. Journal of Biological Regulators and
Homeostatic Agents 15: 1-13, 2001).

We have performed several flow analyses on CD34+ cells purified by the
Miltenyi device and as Paul indicated, the presence of the paramagnetic
microbeads on the selected cells does not affect the light scatter
properties (at least) of the cells.  Indeed, the Miltenyi beads are so
small that they can only be visualised (I am told) by electron
microscopy.  In our experience, we regularly see in excess of 97% purity
of CD34+ cells with this device.  Since we are using this device in
haplo-identical allo-transplant studies, we also interested in
enumerating the residual CD3+ T cells in the selected samples.  To do
this we perform simultaneous absolute CD34+ cell and CD3+ cell
enumeration in a single tube using a variation of the single platform
ISHAGE/CPC protocol (Enumeration of CD34+ Hematopoietic Stem and
Progenitor Cells. Current Protocols in Cytometry Unit 6.4.1-6.4.22,
199).  Our experience indicates that very few CD3+ cells are found in
the CD34+ fraction;  indeed data thus far shows that considerably less
than 10e5 CD3+ cells/Kg patient weight end up in the graft!

Examples (using either Beckman-Coulter or BD Biosystems instruments) of
how these analyses are performed using Beckman-Coulter's Stem-Kit
(CD45FITC, CD34PE and Flow Count beads) supplemented with CD3PE:Cy5  can
be found at the ISHAGE web-site
(www.ishage.org/committees/Committees/Graft_Evaluation/graft.htm).

A few final words of caution;  if you hope to obtain any reliable flow
data whatsoever on CD34+ cells selected with the Miltenyi device, it is
very important to keep the selected CD34+ cell fraction cold (on ice)
from the moment it is eluted from the column, through the staining
proceedure and until the sample is anlaysed by flow. Failure to follow
these simple guidelines will almost certainly result in the generation
of large aggregates of CD34+ cells, consequent to the upregulation of
adhesion molecules on the CD34+ cells.  The latter in turn is due to the
fact that class II (and class I) CD34 antibodies stimulate a
metabolism-dependent upregulation of adhesion molecule expression.  The
presence of aggregates destroys the ability of any flow method, whether
based upon 'two platform' (%CD34+ from cytometry multiplied by the
absolute leukocyte count from a hematology analyser) or 'single
platform' (bead-based absolute CD34+ cell counting) to accurately
enumerate the selected cells.  Because of aggregates, viability
assessments are also futile since for example, a single dead cell within
an aggregate of cells will result in all cells in the aggregate being
excluded from analysis. However, in the allotransplant setting, since
the residual CD3+ cells do not get trapped in the CD34+ cell aggregates,
it is possible, using single platform methods, to accurately assess the
absolute CD3+ cell content in the graft.

I hope this helps.

D. Robert Sutherland,
Department of Medical Oncology and Hematology
Princess Margaret Hospital,
The University Health Network,
Toronto.



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