Streptavidins --- and MHC tetramers too!

From: Mario Roederer (Roederer@DrMR.com)
Date: Mon Feb 28 2000 - 16:04:11 EST


Charles...  Your answer is a bit off...

There are four biotin-binding sites on any single avidin molecule;
four biotins will bind to a single streptavidin (SA).

In the case of biotinylated antibodies, it is theoretically possible
that many conjugated SAs could bind a single multiply-biotinylated
antibody.  In reality, the number of SAs that can fit around a single
antibody is probably pretty small, and when the SA is conjugated to
PE (which is huge) or APC (also large), this number becomes even
smaller (maybe only 1 or 2).  Hence, the amplification noted for
biotin-SA systems is theoretically best for FITC-avidin (or other
small fluorochromes, such as Cy3, Cy5, TexasRed, Alexa, etc.).

That said, why is it that amplifications with SA-PE or SA-APC can be
much more than 3x when it is sterically nearly impossible that even 3
SAs are binding a single IgG?  The answer is that PE-SA and APC-SA
are almost never simple complexes of 1 SA with 1 PE (or APC).  While
such 1:1 complexes can be made (and are commercially available), most
manufacturers sell complexes that are mixtures of much larger
multimers--e.g., 2:2, 3:3, 4:4, ....  This is because of the
chemistry--it is easier to manufacture larger complexes than 1:1
complexes.  And customers prefer these "high order" complexes!  Why?
Because for a single biotin, you can now have a large multi-avidin/PE
complex that has as many as 3 or more PE molecules.  Binding only two
of these complexes to a single antibody can increase fluorescence
6-fold.

(Incidentally, this is why the name "tetramer" for the MHC-HLA
complexes first made at Stanford is a misnomer.  These "tetramers"
are probably complexes that include as many as a dozen
HLA-molecules--"MHC Multimer" is a far more accurate term.
Unfortunately, the term "tetramer" has become so common as to be
irreplaceable...  however, it is important to realize that these are
large-order complexes, because binding studies that purport to
measure affinity become far less meaningful (if any meaning is left)
due to the high order valency of these complexes).

For those interested in more amplification  than the SA-biotin system
(or rather, interested in more fluorescence signal per antigen), you
might want to consider a system devised by Peter Lansdorp (at the
Terry Fox Cancer Center in Vancouver).  He isolated anti-PE
monoclonal antibody, and conjugated it to biotin.  Thus, the sequence
of steps is:

(1) Biotinylated primary
(2) Streptavidin-PE
(3) Biotinylated anti-PE (binds to the SA-PE that is bound to primary)
(4) Strepatavidin-PE

and repeating steps (3) and (4) as many times as you wish... making
bigger and bigger complexes.  Using 3 rounds, we saw amplifications
of about 5x over a single round (but didn't really try to optimize it
too much).  It's a bit painful because of the number of
staining/washing steps involved, but for really rare antigens, it may
just do the trick.

mr

At 1:16 PM -0600 2/25/00, ckuszyns@UNMC.EDU wrote:
>I think your question may be a bit off.  the object of using the Biotin
>-avidin system is to be able to label a primary antibody on the cell
>surface.  You do not use a secondary antibody rather avidin conjugated
>to a
>fluorochrome.
>
>      The theoretical increase in fluorescence that is tauted for this
>complex is based on the chemistry of biotin.  the biotin molecule is
>capable of binding several (I believe 7) avidin molecules.  This is what
>gives you the increased signal since now every biotin molecule on your
>primary antibody is capable of binding 7 molecules of avidin ie 7
>fluorochrome molecules.  This is often more molecules than are attached
>to
>the secondary antibodies used for primary detection.
>
>      One should remember however, that more is not always better.
>Fluorescent molecules may be quenched when in close proximity to other
>fluorescent molecules and therefore the net result may be lower intensity
>signals.
>
>      We have used biotinylated antibodies in three and four color
analyses
>since this gives us the option to use the second laser to detect the
>avidin
>binding using APC.  in our hands, the biotin avidin antibody staining is
>often at least 1 log brighter than the same antibody directly conjugated
>to
>the same fluorochrome.
>
>      There are clearly experts in this society who have a better
>understanding of this area than I so you will want to assess all
>answers to
>this question.
>
>Charles A. Kuszynski, Ph.D.
>Assistant Professor/Director
>University of Nebraska Medical Center
>986495 Nebraska Medical Center
>Cell Analysis Facility, WH 3024
>Omaha,  NE 68198-6495
>402.559.6267 voice
>402.559.4077 fax
>ckuszyns@unmc.edu



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