Re: Para- or not-formaldehyde?

From: Min Ku (min.ku@zoi.unibe.ch)
Date: Wed Jun 09 1999 - 04:55:05 EST


Hello Unni and other FCers,
I know everyone says one should always make up fresh paraformaldehyde each
time, but I make up a big batch of 10% paraformaldehyde (from powder) in
PBS, pH it, aliquot it, and freeze the aliquots at -20°C.  I make up the
aliquot size so that each aliquot has to be thawed and refrozen only a few
times.  So far, this has been fine for my applications (immunofluorescence
and flow cytometry one time) and I use 0.5% to 4% paraformaldehyde.  After
I take out the required amount of PF from the 10%stock, the aliquot goes
back in the freezer until the next experiment.

Sincerely,
Min
At 10:21 07.06.99 +0000, Unni Hadeland wrote:
>
>Para- or not-formaldehyde?
>
>I`ve learned that when you dissolve 1g of solid paraformaldehyde in 10 ml
PBS 
>by extensively heating (boiling) and shaking you get 10% fresh
paraformaldehyde
>which at 4% is perfect for fixing cells for Flow cytometry if used whithin
for 4
>days, then you have to make a new fresh one. By reading the e-mails here, I
>understand what I really have is hydrolysed paraformaldehyde, i.e.
formaldehyde.
>But will it be completely hydrolysed? Or do I have to by the solution of
>formaldehyde containing 10-15% methanol? Or the methanol-free commercially
>available formaldehyde? (Why is the commercially made "ultrapure"
formaldehyde
>fresh/unpolymerized for one year, whereas the home-made hydrolysed
>paraformaldehyde (i.e. formaldehyde) is fresh for only 4 days?)
>
>Thanks much!
>
>Unni Haddeland
>Research Laboratory
>Akershus College
>Ringstabekkvn 105
>1365 Bekkestua
>NORWAY
>
Min Ku, Ph.D. 
c/o Schuemperli Lab
University of Bern
Zoology Institute
Baltzerstr. 4
3012 Bern
Switzerland
phone: 031 631 4681
email: min.ku@zoi.unibe.ch



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