Re: Annexin V and Ca++?

From: Derek Davies (daviesd2@icrf.icnet.uk)
Date: Wed Jan 28 1998 - 06:58:40 EST


Hi Jan,

HL60 is a nice cell line for checking whether your apoptotis detection
system is working, and I have used these cells successfully with the
Annexin technique. As you say you are seeing a sub-G1 peak, I would also
expect you to see a significant amount of apoptotic and dead cells by the
Annexin technique. To induce apoptosis I would usually use 50ug/ml
etoposide or 100ug/ml camptothecin for about 4 hours. Also dont forget
that you are looking at a "snapshot" of the cells at the particular moment
of analysis and the percentages of 'apoptotic' cells found by different
methods of analysis may not be identical.

The binding of Annexin to externalised PS residues is calcium-dependent,
but if you are using a kit, the buffers supplied should be OK. If not I
would use a buffer of 10mM HEPES, 140mM NaCl and 2.5mM CaCl2 (pH7.4). Wash
your cells in this prior to the Annexin staining (Annexin at a
concentration of 2.5ug/ml).


As for your other question, you could detect PI in the FL3 channel, but
there will still be a slight compensation problem of the PI into FL1 and
also the FITC into FL3. This can be compensated but it may not be
immediately obvious how to do it (depending on your machine). And
certainly if you wanted to use FL2 for a PE label you would encounter
difficulty.

Hope this helps!

Derek


 On Mon, 26 Jan 1998, Jan Vondracek wrote:

> 
> I am a complete novice in this field. I work mostly on HL-60 cells. I
> just started to use annexin-V-FITC to detect apoptotic cells and I am
> not very happy with results. In fact, I can detect only about 1% of
> apoptotic cells in my positive control (treated with etoposide), while I
> know that there should be around 30% (determined morphologically under
> microscope and judging from sub-G1 peak).I get only small double
> positive and double negative (over 90%) populations. I know that various
> producers of annexin recommend different buffers with different CaCl2
> concentrations. Could this be the reason of poor annexin staining? My
> second question is perhaps trivial. Why not to use FL3 to detect PI
> positive cells when discriminating apoptotic and necrotic cells - I
> could avoid any compensation error? Is there any problem that I do not
> know about?

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