Re: Annexin V and bcl-2 staining versus azide buffer

From: Lisa Gale (lisa.gale@adelaide.edu.au)
Date: Tue Jul 18 2000 - 20:20:56 EST


Hi Karim, funny you should ask about these issues, as I was wondering
myself just the other week.

I have done one experiment to test the effect of azide (0.04% in wash
buffers) on annexin staining in lymphocyte populations, and it seems
that the presence of azide slightly reduces the number of
annexin-positive cells (27% reduced to 19%). However, as I said, this
was only one sample, so I wouldn't put too much weight on it. (although
I do have a reference showing that azide inhibits apoptosis in Jurkat
cells, so there may be something to this...?)

With regard to fixation in PFA, I have found that dissolving the PFA
(1%) in calcium-containing annexin binding buffer gives good fixation
(scatter profiles are as expected), and I see approximately what I would
expect in terms of annexin staining, although I am yet to compare fixed
cells with un-fixed cells. However, when I used 1%PFA in PBS, the
scatter profile was a mess, and I couldn't gate my lymphocyte
population. I think the calcium buffer reacted somehow with the PFA/PBS,
as there was a white precipitate in my tubes.

Sorry it's all a bit vague, but I hope this helped in some sort of
way...

Lisa


Karim Vermaelen wrote:
>
> Hi everybody,
> We're doing Annexin staining on subsets of lymph node cells obtained
> after collagenase/edta digest. We use Annexin V-PE or
> anti-bcl-2-PE(Pharmingen) in combination with 2 MoAb markers (in FITC
> and RPECy5). I have several nagging questions:
> 1. This may sound quite trivial, but was is the influence of SODIUM
> AZIDE (as in your average FACS washing/staining buffer) on the final
> Annexin staining? I could leave out the azide in the washing buffer, but
> it's still present in minute quantities in the MoAb dilutions used prior
> to the Annexin... any effect on cell apoptosis?
> 2. During staining of such cell suspensions with the MoAbs, we
> preferably use a staining buffer containing 5mM EDTA (to avoid
> lympho-APC reaggregation). Of course I use the Ca-rich Annexin binding
> buffer for the final step, but does the previous presence of EDTA have
> any lingering effect on the quality of the Annexin staining?
> 3. How critical is temperature for the Annexin staining?
> 4. Same thing for bcl-2 staining: how is it influenced by azide?
> 5. Finally, is PFA fixation beneficial or detrimental to the quality of
> Annexin V staining?
>
> Any answers or comments will be greatly appreciated and will help others
> as well I hope!
>
> Karim Y. Vermaelen
> Resp. Diseases, Pulmonary Immunology
> Ghent University Hospital, Belgium

--
Lisa M Gale
Department of Microbiology & Immunology
University of Adelaide
ph  +61 8 8303 4630
fax  +61 8 8303 4362
email lisa.gale@adelaide.edu.au



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